Hanna-instruments HI 83214 Uživatelský manuál Strana 52

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Phosphorus, Acid Hydrolyzable
Remove the cap from a Reagent Vial.
Add exactly 5.0 mL of sample to the vial, while keeping the vial at a
45-degree angle.
Replace the cap and mix by inverting the vial a couple of times.
Insert the vial into the reactor and heat it for 30 minutes at 150 °C.
At the end of the digestion place the vials carefully in the test tube rack and
allow to cool to room temperature.
Warning: The vials are still hot, be careful when handling them.
Select the
Phosphorus,
Acid Hydrolyzable
method following one of the procedures described in the
“Method Selection” section (see page 15).
Remove the cap from the vial and add exactly 2.0 mL of
Sodium Hydroxide (NaOH) Solution 1.20 N, while keeping
the vial at a 45-degree angle.
Replace the cap tightly and mix by inverting the vial a
couple of times. This is the blank.
Place the vial into the holder and push it completely down.
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