Hanna-instruments HI 83266 Uživatelský manuál Strana 13

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Calcium Hardness
CALCIUM HARDNESS
SPECIFICATIONS
Range 0 to 500 mg/L (as CaCO
3
)
Resolution 5 mg/L
Accuracy ±10 mg/L ±5% of reading at 25 °C
Typical EMC ±5 mg/L
Deviation
Light Source Tungsten lamp with narrow band interference filter @ 525 nm
Method Adaptation of the
Standard Methods for the Examination of Water and Wastewater,
18
th
edition,
Calmagite method. The reaction between calcium and reagents causes a
reddish-violet tint in the sample.
REQUIRED REAGENTS
Code Description Quantity
HI 93720A-0 Ca & Mg indicator 0.5 mL
HI 93720B-0 Alkali solution 0.5 mL
HI 93720C-0 EGTA solution 1 drop
REAGENT SETS
HI 93720-01 Reagents for 100 tests
HI 93720-03 Reagents for 300 tests
For other accessories see page 46.
MEASUREMENT PROCEDURE
Select the
Calcium Hardness
method using the procedure
described in the
Method Selection
section (see page 15).
Rinse a graduated beaker several times with deionized
water, fill a 1 mL syringe with the sample, and inject
0.5 mL into the beaker. Fill the beaker up to the 50 mL
mark with hardness-free water.
Add 0.5 mL of HI 93720A-0 Calcium indicator solution
and swirl to mix.
Add 0.5 mL of HI 93720B-0 Alkali solution and swirl to
mix. Use this solution to rinse 2 cuvettes before filling
them up to the 10 mL mark.
Calcium Hardness
Add 1 drop of HI 93720C-0 EGTA solution to one cuvette (# 1), replace
the cap and invert the cuvette several times to mix. This is the blank.
Place the blank (# 1) into the holder and close the lid.
Press the Zero key. The meter will show “-0.0- when the meter is zeroed and ready for
measurement.
Remove the blank and insert the second cuvette (# 2) into
the instrument.
Press Read to start the reading. The instrument displays concentration in mg/L of calcium hardness,
as CaCO
3
.
Press s or t to access the second level functions.
Press the Chem Frm key to convert the result in mg/L of Calcium (Ca).
# 1 # 2
# 1
# 1
# 2
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